Mechanical Micro and Nano properties

The immense applications of coatings in miniaturized components and devices, together with the needs to determine the elastic and plastic properties of materials at the nanometric scale, have led to an increasing development of technologies based on nanoindentation. This technology is gaining more and more followers every day, especially specialists in the study of materials, both in academic and industrial fields and all those related to the mechanical characterization of materials and devices in small volumes.
Nanoindentation is a hardness test carried out at the nanometer length scale. Conventional methods for obtaining the hardness value of a material are based on the optical measurement of the residual trace that remains on the sample after applying a normal load to it. Said load is applied using a diamond indenter with a pyramidal geometry (Vickers or Knoop). The hardness value for said material is calculated by dividing the applied load by the area of the residual imprint.
An indentation measurement is called nanoindentation when the size of the residual trace is too small to be accurately resolved by light microscopy. This is often the case in thin film hardness measurements where very low loads (tenths of mN) must be used to avoid substrate influence. Nanoindentation measurement involves continuous recording of the indenter displacement (depth) and the applied load.
Instrumental Facilities
Nanoindenter XP, Manufacturer: NanoMTS (USA)
Technical Specifications
- Simple indentation essay
- Automated testing. Programming of up to 500 indentations per display.
- Tests involving multiple partial loads and unloads
- Simple scratch tests
- Multiple scratch tests, with different passes in different positions
Indentation Head
- Displacement resolution 0.01 nm
- Percorrido da punta de indentado 2 mm
- Maximum Penetration Depth 500µm
- Maximum load 500 mN
- Resolution in Forza 50 nN
- Motorized and software-controlled XE manipulation table via Rato. Working surface 90×100 mm. Position accuracy: 1.5 µm
- Horizontal position of the samples / Vertical indentation system
CONTINOUS STIFFNESS MEASUREMENT (C. S.M.)
- Continuous force oscillation in the range of 0.05 to 300 Hz
- Force range: 0.1 µN to 300 mN
- Program for dynamic models of dynamic response characterization (Frequency Range: from 0.1 to 2000 Hz)
HIGH-RESOLUTION XY TABLE
- 3D images of the indentation area
- Topographic measurements of the surface
OPTICAL DISPLAY SYSTEM
- Objectives 4X and 40X
- Video camera: 5″ CCD, 768 H x 494V resolution, 10-bit chip
- CCD coupled to Obxectivo
Aplicacións
- Materials Science: Characterization of metal alloys, technical ceramics, and advanced composites.
- Environmental & Biomass: Biomineralization studies on shells, corals, and wood (dry samples).
- Coatings & Thin Films: Evaluation of PVD/CVD layers, varnishes, paints, and electroplated coatings.
- Microelectronics: Quality control of silicon wafers, microsensors (MEMS), and integrated circuits.
- Biomedical: Mechanical analysis of mineralized tissues (bone, dental enamel) and implant materials.
- Tribology: Assessment of wear resistance, friction, and surface mechanical integrity.
- Polymers & Plastics: Determination of elastic properties and hardness in engineering polymers.
- Geology & Mining: Mechanical characterization of minerals, rocks, and shales.
- Optics: Evaluation of technical glass, lenses, and anti-scratch screen coatings.
- Process Control: Verification of heat treatments, welding zones, and surface hardening.
Sample requirements
- The samples must be in good condition and therefore must not contain traces of grease, oils, or any composition that endangers the integrity of the equipment and must be non-toxic or harmful.
- Do not handle the surface of the samples with bare hands. Always wear powder-free nitrile gloves. Our recommendation, in the case of a solid sample, is that before bagging the sample in the plastic bag, it should be protected with aluminium foil (commonly used).
- Samples should be of the appropriate size (dimension) for the technique…Samples exceeding the limits should be cut. It is recommended to contact the technical staff of the Service if there are doubts about the dimensions.
- When the samples are identical on both sides, the user must indicate with a mark the side of interest. If the samples are in powder form, they can be sent in a properly sealed and identified eppendorf vial.
- Upon completion of the work, the samples will be returned to the user in the way is registered on the service form. Samples not delivered to users will be kept at the Service for a stablish period. After this time, the samples will be disposed of as laboratory waste.
More information
Carmen Serra Rodríguez – Tatiana Padín Gómez – Paula Barbazán Martín
+34 986 813 882 – Fax: 986 812 135
cserra@uvigo.es – tatiana.padin@uvigo.es – pbarbazan@uvigo.es

